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The sections on C-13 NMR and proton NMR are written so that they are entirely independent of each other. Obviously I have no way of telling whether you need one of these or both - and if both, what order you need to do them in. That means that you will find quite a lot of duplication in the "Background" pages for both techniques.
If you have a choice, start with C-13 NMR. The spectra are a lot easier to interpret!
C-13 NMR
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Background to C-13 NMR. . .
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An explanation of how a C-13 NMR spectrum arises, and the meaning of the term "chemical shift".
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Interpreting C-13 NMR spectra . . .
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How a C-13 NMR spectrum gives you information about the structure of a molecule.
Proton NMR
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Background to proton NMR. . .
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An explanation of how a proton (1H) NMR spectrum arises, and the meaning of the term "chemical shift".
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Low resolution NMR spectra . . .
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How a low resolution NMR spectrum is used to identify where the hydrogen atoms in a molecule are. Read this before you go on to high resolution spectra.
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High resolution NMR spectra . . .
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Looks at the additional information which you can get from a high resolution NMR spectrum.
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Integrator traces . . .
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How to find the ratio of the numbers of differently placed hydrogen atoms from an integrator trace.
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